PILODIST SP1000CC

WIPED FILM MOLECULAR DISTILLATION SYSTEM

Wiped thin film short path distillation system for botanical applications.

The short path distillation system is designed for distillation of thermally sensitive products under vacuum. The system is used for organic products of thermic instability, high molecular weight and high viscosity at operating temperatures.

The evaporation surface consists of a vertical glass cylinder, double mantled and heated by circulating thermal oil. The product is being spread to a thin film on the inner surface of the evaporator by means of rotating PTFE wiper elements. These wipers are being pressed to the inner wall of the surface where they produce a thin film with a continuous distribution of the liquid film. The condenser is vertically arranged in the centre of the glass evaporator, tempered by liquid flow, to reduce the distance for the vapours to prevent any pressure drop by huge transfer space. This technology enables the operation at extreme high vacuum to reduce the boiling point of thermal sensitive products like botanical extracts without decomposition.

The rotating wiper basket is made of stainless steel AISI 316 and equipped with PTFE (Teflon) roll wipers.

SP 1000 CC is offered as a turn-key system including complete vacuum accessories, three high capacity thermostats to temper feed-vessel, inlet line, evaporator and the condenser including outlet line and fully tempered, vacuum tight, dosing and discharge pumps The residue outlet is tempered by an electrical heating circuit to prevent solidification of very heavy, waxy residues.

TECHNICAL DATA

Operating temperature:up to 200°C (250…350°C upon request)
Vacuum down to:< 1 x 10-5 Torr abs.
Feed range:approx. 1000 – 4000 ml/h, dep. on application (max. 7000ml/h)
Evaporator surface:~1000cm², short path
Evaporator MOC:borosilicate glass & AISI 316 stainless steel
Feed vessel:5000 ml, graduated
Product receivers:variable (2 x 5000ml in scope of supply)
Speed range of stirrer:30…1000 rpm
Dimensions (w x h x d):1750 x 2280 x 820 mm
Electrical Supply:230/400V 25A 3L+N+PE (50Hz or 60Hz available)

Detailed description of voltages and corresponding currents are available upon request.


SPECIAL ADVANTAGES OF THE P1000CC:

Unique Hybrid Evaporator
  • Combines all the positive characteristics of glass and stainless steel
  • Full visibility of the process
  • Reliable and precise
  • Lowest tolerances in the market (no welding, no forming)
  • Easy cleaning
  • lowest maintenance & repair costs due to changeable glass-cylinders
  • complete heated inlet and outlet lines
  • Lowest hold up due to extreme compact design
High capacity glass condenser
  • Reliable and strong design
  • Easy removable for cleaning
  • Full visibility
  • Complete tempered
  • Maximized surface and minimized distance to the evaporator
Precise Vacuum control system
  • Digital vacuum controller for high reproducibility
  • Double vacuum sensor system
  • No problems with incondensable vapors due to high capacity oil free scroll vacuum pump (15m³/h)
  • Vacuum line in huge diameter for maximum performance and easy cleaning – Automatic safety circuit for diffusion pump control
  • Double condensate receiver system to separate light ends
  • High capacity diffusion pump (65l/s → 234m³/h) with oil level indicator
  • Supersized vacuum cold-trap for outstanding vacuum performance
  • Cold-Trap with drain nozzle for easy maintenance 
  • Optional electrical immersion cooler down to -90°C (no dry ice needed)
Vertical design for optimized product flow without hold-up in useless pumping lines
Hermetically sealed, high vacuum tight, tempered gear pumps for fully continuous operation
Complete tempered discharge system without any solidification of heavy residues
Sophisticated control cabinet for easy handling with “CULUS” approval
All heating/cooling circuits with maximized diameter and minimized length for optimized heat transfer
Tool-less maintenance of wiper basket and drive motor
The SP1000CC got the possibility to be upgraded later on to the fully continuous dual-stage-system SP1000CC-DUAL